Determination of phase transitions in gutta-percha by differential thermal analysis.
نویسندگان
چکیده
Pure gutta-percha was heat-treated in a differential thermal analyzer. The high melting form crystallized on cooling when gutta-percha was heated to 70 C or less. Above 74 C, crystallization into the low melting form predominated. Either polymorph can be selectively crystallized by control of the heat-treatment temperature before cooling.
منابع مشابه
Chemical composition and thermal behavior of five brands of thermoplasticized gutta-percha
OBJECTIVE The aim of this study was determine the chemical composition and thermal behavior of Thermafil (TH), Microseal Cone (MC), Microseal Microflow (MF), Obtura (OB) and Obtura Flow (OF). In addition, their thermal behavior in response to temperature variations was studied by differential scanning calorimetry (DSC) to determine the temperature at which gutta-percha switches from the beta to...
متن کاملVarious methods of Gutta-Percha Removal on the apical Seal-an
BACKGROUND: It's often necessary to fabricate a post & core for restoration of an endodontically treated tooth. One of the important step in post & core technique is preparation of post space by removal of gutta-percha from root canal leaving 3 5mm at the apex, so that the apical seal is not disturbed. Objective of this study to evaluate effect of various methods of gutta-percha removal on apic...
متن کاملShear modulus and thermal properties of gutta percha for root canal filling.
The purpose of this investigation was to investigate the rheological properties of four commercially available gutta perchas for root canal filling. The relaxation modulus [Gr(0): instantaneous shear modulus] and specific volume of their materials were examined. In addition, the quantity of heat was also studied by differential scanning calorimeter. In a lower temperature range than the first-o...
متن کاملEffect of Post-Space Preparation on Apical Seal of Endodontically Treated Teeth
ABSTRACT By restoration of pulpally exposed teeth with root canal therapy edentulous areas and neighbouring teeth displacement can be avoided. Prefabricated posts may be used for crown restoration of these teeth. For the preparation of root canal for post placement, Gutta percha should be removed by means of mechanical, thermal and chemical agents. To study the amount of apical leakage in vit...
متن کاملبررسی اثر برخی افزودنی ها بر انتقالات فازی و رفتار حرارتی آمونیوم نیترات
Ammonium nitrate (AN) is widely used in fertilizers, civilian explosives and military explosives. Due to crystalline phase transitions and density changes of AN in the ambient conditions, its usage as oxidizer in solid propellants has some limitations as compared to ammonium perchlorate (AP). Several methods have been introduced to overcome these problems. In the present paper, the phase transi...
متن کاملذخیره در منابع من
با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید
برای دانلود متن کامل این مقاله و بیش از 32 میلیون مقاله دیگر ابتدا ثبت نام کنید
ثبت ناماگر عضو سایت هستید لطفا وارد حساب کاربری خود شوید
ورودعنوان ژورنال:
- Journal of dental research
دوره 56 12 شماره
صفحات -
تاریخ انتشار 1977